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Synlett 1994; 1994(1): 61-62
DOI: 10.1055/s-1994-22738
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A Novel Synthesis of Methyl [6-(α-methoxyimino)ethyl]salicylate

Kazuto Umezu* , Keisuke Isozumi, Tomonori Miyazaki, Masatoshi Tamaru, Fumiaki Takabe, Naoshi Masuyama, Yoshikazu Kimura
  • *Research and Development Department, Ihara Chemical Industry Co., Ltd., Fujikawa-cho, Ihara-gun, Shizuoka 421-33, Japan
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Publication Date:
22 March 2002 (online)

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A highly efficient synthesis of the title compound was accomplished by employing the directed ortho lithiation in toluene at room temperature and methoxyiminodeacetallization as key steps from 3-hydroxyacetophenone.